MTech Synthesis And Characterization Lab syllabus for 1 Sem 2018 scheme 18INTL16

Module-1 Lab 40 hours

1. Verification of Beer Lombard’s Law

2. Synthesis of Au/Ag metal nanoparticles by Chemical reduction method, UV-Visible absorption studies of the Au/Ag metal nanoparticles

3. Synthesis of ZnO nanoparticles by hydrothermal method and Optical absorption spectra of the ZnO; Band gap estimation from the band edge

4. Synthesis of TiO2 nanoparticles by Solvothermal method and Photocatalytic degradation property analysis

5. Synthesis of ceramic BaTiO3 nanomaterial by combustion process and their crystal structure identification by X-ray diffraction studies

6. Synthesis of ceramic SrTiO3 nanomaterial by Sol-Gel method and their Size Calculation Scherer’s law by X-ray diffraction pattern

7. Surface functionalization or modification of Al2O3 metal oxide nanoparticles with organic reagents. Surface modification confirmation by dispersion in binary solvent (Organic-Aqueous) system.

8. Synthesis of Fe2O3/Mn3O4 nanoparticles by Co-precipitation method

9. Surface functionalization or modification of Fe2O3 metal oxide nanoparticles with organic reagents. Surface functional group identification by FTIR measurement

10. Synthesis of ZnS/MoS nanoparticles by microwave Solvothermal method followed by size and morphology analysis

 

Course Outcomes:

The Student will be able

1. Design the experiments to synthesize desired nanoparticles.

2. Prepare size and morphology controlled nanostructures.

3. Characterize the structural, optical and surface chemistry of the synthesized sample.

4. Relate the size and structure of materials to properties